楚文娟,张文洁,田海英,高明奇,赵声辰,冯衍闯,张峻松.烟用甜味接装纸中纽甜的衰减特性[J].包装工程,2021,42(23):130-135.
CHU Wen-juan,ZHANG Wen-jie,TIAN Hai-ying,GAO Ming-qi,ZHAO Sheng-chen,FENG Yan-chuang,ZHANG Jun-song.Attenuation Characteristics of Neotame in Sweet Tipping Paper for Cigarette[J].Packaging Engineering,2021,42(23):130-135. |
| 烟用甜味接装纸中纽甜的衰减特性 |
| Attenuation Characteristics of Neotame in Sweet Tipping Paper for Cigarette |
| 投稿时间：2021-01-12 |
| DOI：10.19554/j.cnki.1001-3563.2021.23.018 |
| 中文关键词: 接装纸 纽甜 衰减量 衰减率 |
| 英文关键词: tipping paper neotame attenuation attenuation rate |
| 基金项目:河南中烟工业有限责任公司科技项目(2020410001340008) |
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| 中文摘要: |
| 目的 考察甜味接装纸中纽甜的衰减特性，为明确纽甜烟用接装纸的贮存期提供参考。方法 设计和制备6个不同纽甜含量的烟用接装纸，并通过高效液相色谱-二极管阵列检测器(HPLC-DAD)法考察存放时间对烟用接装纸中纽甜的衰减情况的影响。结果 该方法在75~500 μg/mL线性良好(r≥0.999)，平均回收率为92.31%~103.75%(RSD=0.35%～2.32%，n=5);1#—3#，4#和6#，5#接装纸的平稳期分别在20~100 d， 20~160 d，80~160 d;在0~100 d，纽甜添加范围为0.47~0.62 mg/g和0.82 ~1.37 mg/g的接装纸衰减率分别在19.15%~33.87%和11.68 %~31.62%;在100~200 d，纽甜添加范围为0.47~0.62 mg/g和0.82~1.37 mg/g的接装纸衰减率分别在42.55%~95.74%，23.36%~65.85%。结论 该方法适用于烟用甜味接装纸中纽甜含量的测定;接装纸中纽甜的平稳期整体随添加量的增加而增加;在0~100 d，接装纸中纽甜含量衰减较缓慢，不同添加量的接装纸衰减率基本一致;在100~200 d，接装纸中纽甜含量衰减较快，衰减率随添加量的增加而降低;纽甜添加范围为0.47~0.62 mg/g的接装纸贮存期在200 d以内;纽甜添加范围为0.82~1.37 mg/g的接装纸贮存期不能确定。 |
| 英文摘要: |
| The work aims to investigate the attenuation characteristics of neotame in sweet tipping paper and provide a reference for clarifying the storage period of neotame tipping paper. Six types of cigarette tipping paper with different neotame contents were designed and prepared, and the effect of storage period on attenuation of neotame in cigarette tipping paper was investigated by high performance liquid chromatography-diode array detector (HPLC-DAD) method. The method had good linearity in the mass concentration range of 75~500 μg/mL (r≥0.999), and the average recovery rate was between 92.31% and 103.75% (RSD=0.35%～2.32%, n=5). 1#~3#, 4# and 6#, 5# tipping paper had a plateau period of 20~100 d, 20~160 d, and 80~160 d respectively. Within 0~100 d, the attenuation rate of the tipping paper with neotame of 0.47~0.62 mg/g and 0.82~1.37 mg/g was between 19.15%~33.87% and 11.68%~31.62%, respectively. Within 100~200 d, the attenuation rate of the tipping paper with neotame of 0.47~0.62 mg/g and 0.82~1.37 mg/g was 42.55%~95.74% and 23.36%~65.85%, respectively. This method is suitable for the determination of neotame content in sweet tipping paper for cigarettes. The stable period of neotame in the tipping paper increases with the increase of the addition content. Within 0~100 d, the neotame content in the tipping paper decays slowly and the attenuation rate of the tipping paper with different addition contents is basically the same. Within 100~200 d, the neotame content in the tipping paper decays fast, and the attenuation rate decreases with the increase of the addition content. The storage period of the tipping paper with neotame in the range of 0.47~0.62 mg/g is within 200 days, while the storage period of the tipping paper with neotame in the range of 0.82 ~1.37 mg/g is still uncertain. |
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